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はちみつに含まれるHMF 定量分析法の開発
https://doi.org/10.24514/00002855
https://doi.org/10.24514/0000285508d53da1-84c5-4d63-874f-114ac02dc788
| 名前 / ファイル | ライセンス | アクション |
|---|---|---|
nfri_report_No74p7-13p.pdf (230.5 kB)
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| Item type | 紀要論文01 / Departmental Bulletin Original Article(1) | |||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|
| 公開日 | 2019-12-20 | |||||||||||
| タイトル | ||||||||||||
| タイトル | はちみつに含まれるHMF 定量分析法の開発 | |||||||||||
| タイトル | ||||||||||||
| タイトル | A new method for the quantification of HMF in honey | |||||||||||
| 言語 | en | |||||||||||
| 言語 | ||||||||||||
| 言語 | jpn | |||||||||||
| キーワード | ||||||||||||
| 主題Scheme | Other | |||||||||||
| 主題 | はちみつ | |||||||||||
| キーワード | ||||||||||||
| 主題Scheme | Other | |||||||||||
| 主題 | HMF | |||||||||||
| キーワード | ||||||||||||
| 主題Scheme | Other | |||||||||||
| 主題 | 前処理法 | |||||||||||
| キーワード | ||||||||||||
| 主題Scheme | Other | |||||||||||
| 主題 | 定量分析 | |||||||||||
| 資源タイプ | ||||||||||||
| 資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||||||||
| 資源タイプ | departmental bulletin paper | |||||||||||
| ID登録 | ||||||||||||
| ID登録 | 10.24514/00002855 | |||||||||||
| ID登録タイプ | JaLC | |||||||||||
| 著者 |
箭田, 浩士
× 箭田, 浩士× 谷中, かおる× 亀山, 眞由美
WEKO
988
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| 抄録 | ||||||||||||
| 内容記述タイプ | Abstract | |||||||||||
| 内容記述 | The method of HPLC sample preparation for 5-hydorxymethyl-2-furfural (HMF) quantification in honey was developed. This method carried out as follows, dilute honey with ethanol/water =70/30 (v/v), centrifuge the solution, and filtrate the centrifugal supernatant with 0.2μm membrane filter. HPLC samples prepared from the filtrate by dilution with water, which were indicated stable analytical values of HMF during one-night(16hrs). This method is useful for routine HMF quantification in honey, because no waste solution containing zinc acetate. We also described the HPLC condition, gradient elution with C18 column/ detection at 254 nm and 284 nm. This HPLC condition make easy to detect the peak which changed from HMF. | |||||||||||
| 抄録 | ||||||||||||
| 内容記述タイプ | Abstract | |||||||||||
| 内容記述 | The method of HPLC sample preparation for 5-hydorxymethyl-2-furfural (HMF) quantification in honey was developed. This method carried out as follows, dilute honey with ethanol/water =70/30 (v/v), centrifuge the solution, and filtrate the centrifugal supernatant with 0.2μm membrane filter. HPLC samples prepared from the filtrate by dilution with water, which were indicated stable analytical values of HMF during one-night(16hrs). This method is useful for routine HMF quantification in honey, because no waste solution containing zinc acetate. We also described the HPLC condition, gradient elution with C18 column/ detection at 254 nm and 284 nm. This HPLC condition make easy to detect the peak which changed from HMF. | |||||||||||
| 書誌情報 |
食品総合研究所研究報告 en : Report of National Food Research Institute 巻 74, p. 7-13, 発行日 2010-03-01 |
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| 出版者 | ||||||||||||
| 出版者 | 農業・食品産業技術総合研究機構 | |||||||||||
| ISSN | ||||||||||||
| 収録物識別子タイプ | ISSN | |||||||||||
| 収録物識別子 | 0301-9780 | |||||||||||
| DOI | ||||||||||||
| 関連タイプ | isIdenticalTo | |||||||||||
| 識別子タイプ | DOI | |||||||||||
| 関連識別子 | 10.24514/00002855 | |||||||||||
| 著者版フラグ | ||||||||||||
| 出版タイプ | VoR | |||||||||||
| 出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||||||||
